化工社化工社 化学情報印刷レポート · 研究参考用
Water → N-decyl galactosylamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Water | HCID 962 | — |
| 反応物 | Decylamine | HCID 8916 | — |
| 反応物 | beta-D-Galactopyranose | HCID 439353 | — |
| 溶媒 | Diethyl ether methanol | HCID 21864698 | — |
| 生成物 | N-decyl galactosylamine | HCID 18656111 | 90% |
反応手順
β-D-galactose (10 g, 1 eq), decylamine (8.7 g, 1 eq), and water (2 g, 3eq) were heated in a reaction flask for 20 min at 80° C. Methanol/ethyl ether (50 v/50 v) was added, the product was filtered, washed with ethyl ether (2×50 ml) and dried, to give a 90% yield.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05362480 |
| 出典データセット | uspto-grants-1994_11 |
| ORD ID | ord-159b09309746474bb577eeb0211f48a2 |
| 出典メモ | uspto-grants-1994_11 |