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Dimethylamine → 5-Nitro-6-dimethylaminoquinoline
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dimethylamine | HCID 674 | — |
| 反応物 | 6-Chloro-5-nitroquinoline | HCID 4070800 | — |
| 生成物 | 5-Nitro-6-dimethylaminoquinoline | HCID 19027869 | — |
反応手順
5-Nitro-6-chloroquinoline, prepared as described by Maneke & Kulka, Organic Reactions, Vol. VII, 59 (1953) and Campbell et al., J. Am. Chem, Soc., 68, 1559 (1946), was allowed to react with dimethylamine to yield 5-nitro-6-dimethylaminoquinoline. This material was converted to the title compound by the procedure described in Example 33.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05362878 |
| 出典データセット | uspto-grants-1994_11 |
| ORD ID | ord-475105343f304126a6e2a6e0be243c30 |
| 出典メモ | uspto-grants-1994_11 |