化工社化工社 化学情報印刷レポート · 研究参考用
Thionyl Chloride → 4'-n-Decylbiphenyl-4-carboxylic acid chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 反応物 | 4'-n-Decyl-4-carboxybiphenyl | HCID 11405011 | — |
| 生成物 | 4'-n-Decylbiphenyl-4-carboxylic acid chloride | HCID 54012389 | — |
反応手順
After 4'-n-decyl-4-carboxybiphenyl (3.10 g) was heated under reflux for 6 hours together with an excessive amount of thionyl chloride, unaltered thionyl chloride was removed by distillation to give about 3 g of 4'-n-decylbiphenyl-4-carboxylic acid chloride.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05364561 |
| 出典データセット | uspto-grants-1994_11 |
| ORD ID | ord-268bbd2b02cb424aa986af4ecfbef9e9 |
| 出典メモ | uspto-grants-1994_11 |