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Water → HCID 67790522、化合物

HRID 2380562
ノート
印刷プレビュー

反応式

HRID 2380562 の反応式
[CH:1]([C:4]1[C:5]([O:16][CH3:17])=[C:6]([CH:10]=[C:11]([CH:13]([CH3:15])[CH3:14])[CH:12]=1)[C:7]([OH:9])=[O:8])([CH3:3])[CH3:2].[OH-].[K+].O.O.O.O.O.O.O.O.S([O-])([O-])(=O)=O.[Zn+2:33]>CO>[CH:1]([C:4]1[C:5]([O:16][CH3:17])=[C:6]([CH:10]=[C:11]([CH:13]([CH3:15])[CH3:14])[CH:12]=1)[C:7]([O-:9])=[O:8])([CH3:3])[CH3:2].[Zn+2:33].[CH:1]([C:4]1[C:5]([O:16][CH3:17])=[C:6]([CH:10]=[C:11]([CH:13]([CH3:15])[CH3:14])[CH:12]=1)[C:7]([O-:9])=[O:8])([CH3:3])[CH3:2]
参加物反応条件実験手順後処理出典と根拠反応ノート

参加物

6

反応物 4

HCID 962Water2 回HCID 14797Potassium HydroxideHCID 62640Zinc Sulfate HeptahydrateHCID 189545872-Methoxy-3,5-di(propan-2-yl)benzoic acid

生成物 1

HCID 67790522HCID 67790522、化合物

試薬・触媒・溶媒 1

HCID 887Methanol溶媒

反応条件

温度
60 °C

実験手順

Five parts of 3,5-diisopropyl-2-methoxybenzoic acid was dissolved in 80 parts of methyl alcohol, followed by the addition of an aqueous solution of 1.3 parts of 96% potassium hydroxide in 10 parts of water. The resulting mixture was heated to 60° C. An aqueous solution of 3.2 parts of zinc sulfate heptahydrate in 10 parts of water was dropped into the resulting mixture over a period of 15 minutes. After the completion of the dropping, the obtained mixture was stirred at that temperature for 2 hours, cooled to a room temperature and filtered to recover a white crystalline precipitate. This precipitate was dispersed in 60 parts of water, washed therewith and filtered. The obtained filter cake was dried to give 4.8 parts of a white crystal. The melting point thereof was 104 to 107° C.

後処理

  1. temperaturecooled to a room temperature
  2. filtrationfiltered
  3. customto recover a white crystalline precipitate
  4. additionThis precipitate was dispersed in 60 parts of water
  5. washwashed
  6. filtrationfiltered
  7. filtrationThe obtained filter cake
  8. customwas dried
  9. customto give 4.8 parts of a white crystal
  10. customthereof was 104 to 107° C.

出典と根拠

ORDレコード
ord-be9b6bc0429c4fb4a61a7f4d75c9dabe
出典データセット
uspto-grants-1994_11
DOI
10.6084/m9.figshare.5104873.v1
特許番号
US05368971

反応ノート

読み込み中…

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