化工社化工社 化学情報印刷レポート · 研究参考用
Glycylglycine → Methacryloylglycylglycine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Glycylglycine | HCID 11163 | — |
| 反応物 | Methacryloyl chloride | HCID 13528 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Methacryloylglycylglycine | HCID 10241886 | 75% |
反応手順
Using Example 1, glycylglycine was reacted with methacryloyl chloride in water at -10° C. After adjustment to a pH of 3, the white slurry was washed with ethanol to remove sodium chloride and water. The product was dried at 80° C. to obtain a good yield (>75%) product with a melting point of 200°-201° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05369142 |
| 出典データセット | uspto-grants-1994_11 |
| ORD ID | ord-86af07b8d12f4df8a95f65f97388eba5 |
| 出典メモ | uspto-grants-1994_11 |