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HRID 2384137作成日：2026年10月27日

Ethyl 2-[(5-amino-1,3,4-thiadiazol-2-yl)sulfanyl]acetate → {5-[3,3-Bis-(4-methyl-cyclohexyl)-ureido]-[1,3,4]thiadiazol-2-ylsulfanyl}-acetic acid

https://huagongshe.com/reaction/2384137

反応式

関与物質

役割名称HCID仕込み量
反応物Ethyl 2-[(5-amino-1,3,4-thiadiazol-2-yl)sulfanyl]acetateHCID 351912—
反応物4-methyl-N-(4-methylcyclohexyl)cyclohexan-1-amineHCID 417228—
反応物{5-[3,3-Bis-(4-methyl-cyclohexyl)-ureido]-[1,3,4]thiadiazol-2-ylsulfanyl}-acetic acid ethyl esterHCID 66871997—
生成物{5-[3,3-Bis-(4-methyl-cyclohexyl)-ureido]-[1,3,4]thiadiazol-2-ylsulfanyl}-acetic acidHCID 57883670—

反応手順

{5-[3,3-Bis-(4-methyl-cyclohexyl)-ureido]-[1,3,4]thiadiazol-2-ylsulfanyl}-acetic acid ethyl ester prepared from bis-(4-methyl-cyclohexyl)-amine and ethyl-2-[5-amino-1,3,4-thiadiazol-2-yl-thio]acetate as described in general procedures (A) and (B). Hydrolysis using general procedure (F) gave the title compound.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US08263634B2
出典データセットuspto-grants-2012_09
ORD IDord-2bd09c67432c49d59b8d628f858581cf
出典メモuspto-grants-2012_09