5-Chlorosalicylic Acid → 5-Chloro-2-hydroxy-N-[2-nitro-5-(trifluoromethyl)phenyl]benzamide

HRID 2384409

反応式

HRID 2384409 の反応式
[Cl:1][C:2]1[CH:10]=[C:6]([C:7]([OH:9])=O)[C:5]([OH:11])=[CH:4][CH:3]=1.[N+:12]([C:15]1[CH:21]=[CH:20][C:19]([C:22]([F:25])([F:24])[F:23])=[CH:18][C:16]=1[NH2:17])([O-:14])=[O:13]>>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([OH:11])=[C:6]([CH:10]=1)[C:7]([NH:17][C:16]1[CH:18]=[C:19]([C:22]([F:25])([F:24])[F:23])[CH:20]=[CH:21][C:15]=1[N+:12]([O-:14])=[O:13])=[O:9]

参加物

3

反応物 2

HCID 94475-Chlorosalicylic AcidHCID 2231003-Amino-4-nitrobenzotrifluoride

生成物 1

HCID 178603085-Chloro-2-hydroxy-N-[2-nitro-5-(trifluoromethyl)phenyl]benzamide収率 8.1%

実験手順

Using 5-chlorosalicylic acid and 2-nitro-5-(trifluoromethyl)aniline as the raw materials, the same operation as the example 16 gave the title compound.

出典と根拠

ORDレコード
ord-6f9ca197cb82442eacf183630fdc0fbb
出典データセット
uspto-grants-2012_09
特許番号
US08263657B2

関連ノート

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