化工社化工社 化学情報印刷レポート · 研究参考用
Ethylenediamine → N~1~-(Pyridin-2-yl)ethane-1,2-diamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethylenediamine | HCID 3301 | — |
| 反応物 | 2-Fluoropyridine | HCID 9746 | — |
| 生成物 | N~1~-(Pyridin-2-yl)ethane-1,2-diamine | HCID 410428 | — |
反応手順
Ethylenediamine (6 g, 0.1 mol) and 2-fluoropyridine (10 g, 0.1 mol) were heated neat at 120° C. overnight. The reaction was cooled and the residue was used in next step without further purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08642624B2 |
| 出典データセット | uspto-grants-2014_02 |
| ORD ID | ord-d13c71bd5af9458eb262afc0d4dc0739 |
| 出典メモ | uspto-grants-2014_02 |