関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Allylamine | HCID 7853 | — |
| 反応物 | Sodium Methoxide | HCID 10942334 | — |
| 反応物 | ethyl 3-(N-vinylformamido)propionate | HCID 19690337 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | N-allyl-3-(N-vinylformamido)propionamide | HCID 19690345 | — |
反応手順
A 100mL stainless steel high pressure reactor was charged with 17.1 grams (0.1 mol) of ethyl 3-(N-vinylformamido)propionate, 5.7 grams (0.1 mol) of allylamine and 0.15 gram of 25% sodium methoxide in methanol solution. The mixture was heated at 90° C. for 3 hours. Subsequent NMR analysis of the reaction mixture showed no conversion of the starting materials.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05728878 |
|---|
| 出典データセット | uspto-grants-1998_03 |
|---|
| ORD ID | ord-e627c68d0c1743fc987ec32e90fb2b64 |
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| 出典メモ | uspto-grants-1998_03 |
|---|
