化工社化工社 化学情報印刷レポート · 研究参考用
2-((4-Chlorophenoxy)methyl)oxirane → Phenyl glycidyl ether
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-((4-Chlorophenoxy)methyl)oxirane | HCID 91515 | — |
| 反応物 | 3-Methyl-2-oxo-2,3-dihydro-benzimidazole-1-carboxylic acid (piperidin-4-ylmethyl)-amide | HCID 67378205 | — |
| 生成物 | Phenyl glycidyl ether | HCID 31217 | — |
| 生成物 | 3-isopropyl-2-oxo-N-(piperidin-4-ylmethyl)-2,3-dihydro-1H-benzimidazole-1-carboxamide | HCID 44249188 | — |
反応手順
The procedure given in Example 104 was followed using 3-methyl-2-oxo-2,3-dihydro-benzimidazole-1-carboxylic acid (piperidin-4-ylmethyl)-amide and 4-chlorophenyl glycidyl ether as a reactant, instead of 3-isopropyl-2-oxo-2,3-dihydro-benzimidazole-1-carboxylic acid (piperidin-4-ylmethyl)-amide and 1,2-epoxy-3-phenoxypropane, to give the title compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08642772B2 |
| 出典データセット | uspto-grants-2014_02 |
| ORD ID | ord-85abc6a52fac467b88b6620e43b0be96 |
| 出典メモ | uspto-grants-2014_02 |