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2,3-Epoxypropyl 4'-methoxyphenyl ether → Phenyl glycidyl ether
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2,3-Epoxypropyl 4'-methoxyphenyl ether | HCID 16646 | — |
| 反応物 | 3-Methyl-2-oxo-2,3-dihydro-benzimidazole-1-carboxylic acid (piperidin-4-ylmethyl)-amide | HCID 67378205 | — |
| 生成物 | Phenyl glycidyl ether | HCID 31217 | — |
| 生成物 | 3-isopropyl-2-oxo-N-(piperidin-4-ylmethyl)-2,3-dihydro-1H-benzimidazole-1-carboxamide | HCID 44249188 | — |
反応手順
The procedure given in Example 104 was followed using 3-methyl-2-oxo-2,3-dihydro-benzimidazole-1-carboxylic acid (piperidin-4-ylmethyl)-amide and glycidyl 4-methoxyphenyl ether as a reactant, instead of 3-isopropyl-2-oxo-2,3-dihydro-benzimidazole-1-carboxylic acid (piperidin-4-ylmethyl)-amide and 1,2-epoxy-3-phenoxypropane, to give the title compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08642772B2 |
| 出典データセット | uspto-grants-2014_02 |
| ORD ID | ord-20f44c5fbb9747ca8b66a6cc25461905 |
| 出典メモ | uspto-grants-2014_02 |