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HRID 2390239作成日：2026年10月26日

3-bromo-N,N-dimethylbenzamide → HCID 58521976、化合物

https://huagongshe.com/reaction/2390239

反応式

関与物質

役割名称HCID仕込み量
反応物3-bromo-N,N-dimethylbenzamideHCID 3335826—
反応物Tert-butyl(4-chloro-2-ethynylphenoxy)acetateHCID 56594381—
生成物HCID 58521976HCID 58521976—

反応手順

Following the general method as outlined in Intermediate 20, starting from (4-chloro-2-ethynyl-phenoxy)-acetic acid tert-butyl ester (Intermediate 3) and 3-bromo-N,N-dimethylbenzamide (Intermediate 180), the title compound was obtained as a brown sticky solid after purification by flash column chromatography (silica), eluting with cyclohexane containing increasing amounts of EtOAc.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US08273769B2
出典データセットuspto-grants-2012_09
ORD IDord-7e477b5d4ae94c7f8f66875eaa2441cd
出典メモuspto-grants-2012_09