Methylamine → Benzyl 3-(methylamino)but-2-enoate
反応式
[C:1]([O:7][CH2:8][C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1)(=[O:6])[CH2:2][C:3]([CH3:5])=O.[CH3:15][NH2:16]>C(O)C>[CH2:8]([O:7][C:1](=[O:6])[CH:2]=[C:3]([NH:16][CH3:15])[CH3:5])[C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1参加物
4
実験手順
To benzyl acetoacetate (29 g, 151 mmol) in ethanol (30 mL) was added methyl amine (33% in ethanol, 7.02 g, 226 mmol). The solution was stirred for 2 hours at room temperature followed by evaporation to yield a yellow oil (˜30 g).
後処理
- customfollowed by evaporation
出典と根拠
- ORDレコード
- ord-fcbee985fa67416690699ca4a74f9300
- 出典データセット
- uspto-grants-2012_09
- 特許番号
- US08273780B2
反応ノート
読み込み中…