化工社化工社 化学情報印刷レポート · 研究参考用
Benzylamine → N-(1,1-Dimethoxypropan-2-ylidene)-1-phenylmethanamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzylamine | HCID 7504 | — |
| 反応物 | Sulfuric acid magnesium salt (1:1) | HCID 24083 | — |
| 反応物 | Pyruvic aldehyde dimethyl acetal | HCID 80650 | — |
| 生成物 | N-(1,1-Dimethoxypropan-2-ylidene)-1-phenylmethanamine | HCID 71380533 | — |
反応手順
12.9 mL 1,1-dimethoxyacetone was added to 10 mL benzylamine in 100 mL petrolether. Magnesiumsulfate was added and the reaction was stirred over night at RT. The mixture was filtered and evaporated to give 18.9 g of the desired product. (M+H)+: 209
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08642774B2 |
| 出典データセット | uspto-grants-2014_02 |
| ORD ID | ord-b3bc05dd952240c8a50ff875b993000c |
| 出典メモ | uspto-grants-2014_02 |