化工社化工社 化学情報印刷レポート · 研究参考用
4-(Trifluoromethyl)phenol → 2-Hydroxy-5-trifluoromethylbenzaldehyde
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-(Trifluoromethyl)phenol | HCID 67874 | — |
| 反応物 | Ethyl acetate hexane | HCID 21226206 | — |
| 生成物 | 2-Hydroxy-5-trifluoromethylbenzaldehyde | HCID 15500988 | 34% |
反応手順
Following the general procedure and FCC purification with 30% ethyl acetate-hexane, 4-trifluoromethyl phenol (10.0 g, 61.7 mmol) gave 2-hydroxy-5-trifluoromethyl-benzaldehyde 27 (3.9 g, 34%) as a pink solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06855695B2 |
| 出典データセット | uspto-grants-2005_02 |
| ORD ID | ord-28e0930bac704493b0adc4c206e0474c |
| 出典メモ | uspto-grants-2005_02 |