関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Acetic Anhydride | HCID 7918 | — |
| 反応物 | (R)-N5-[amino(nitroimino)methyl]-N-[(4-hydroxyphenyl)methyl)-ornithinamide | HCID 136381090 | — |
| 溶媒 | Acetic Acid | HCID 176 | — |
| 生成物 | (R)-N2-Acetyl-N5-[amino(nitroimino)methyl]-N-[(4-hydroxyphenyl)methyl]-ornithinamide | HCID 136381103 | — |
反応手順
0.3 g (0.925 mMol) of (R)-N5 -[amino(nitroimino)methyl]-N-[(4-hydroxyphenyl)methyl]-ornithinamide were dissolved in 3 ml of glacial acetic acid and after the addition of 3 ml (0.032 Mol) of acetic anhydride the mixture was heated to a reaction temperature of 50° C. for 30 minutes. The product remaining after the volatile components had evaporated off was further processed without purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05807875 |
|---|
| 出典データセット | uspto-grants-1998_09 |
|---|
| ORD ID | ord-31ea9a0506fa40a8941c09e0e2b196c5 |
|---|
| 出典メモ | uspto-grants-1998_09 |
|---|
