化工社化工社 化学情報印刷レポート · 研究参考用
Indole-4-carboxaldehyde → 1-[2-(Thien-2-yl)ethyl]indole-4-carbaldehyde
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Indole-4-carboxaldehyde | HCID 333703 | — |
| 反応物 | 2-(2-Thienyl)ethyl methanesulphonate | HCID 3047723 | — |
| 生成物 | 1-[2-(Thien-2-yl)ethyl]indole-4-carbaldehyde | HCID 18973449 | 39.1% |
反応手順
The same procedures used in Example 1 were repeated except for using 435 mg of indole-4-carbaldehyde and 680 mg of 2-(thien-2-yl)ethyl methanesulfonate instead of the benzyl bromide used in Example 1 to give 299 mg of 1-[2-(thien-2-yl)ethyl]indole-4-carbaldehyde as an orange-colored oily substance. The yield thereof was found to be 39%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05811439 |
| 出典データセット | uspto-grants-1998_09 |
| ORD ID | ord-4573cf993a3f4246baa35f49df38e063 |
| 出典メモ | uspto-grants-1998_09 |