Hydrochloric Acid → 3-Amino-4-phenyl-2-butanone hydrochloride (1:1)
反応式
C([NH:4][CH:5]([CH2:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1)[C:6](=[O:8])[CH3:7])(=O)C.[ClH:16]>C(O)C>[ClH:16].[NH2:4][CH:5]([CH2:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1)[C:6](=[O:8])[CH3:7]参加物
4
実験手順
A mixture of 3-acetylamino-4-phenyl-2-butanone (12.5 g), 6N HCl (50 ml) and ethanol (50 ml) was stirred under refluxing conditions for 18 hours. The reaction mixture was concentrated under reduced pressure to yield 3-amino-4-phenyl-2-butanone hydrochloride (9.8 g, 81%).
後処理
- concentrationThe reaction mixture was concentrated under reduced pressure
出典と根拠
- ORDレコード
- ord-c78edbd5751a4a8eba828c8a9ca9e654
- 出典データセット
- uspto-grants-1996_02
- 特許番号
- US05489602
反応ノート
読み込み中…