Potassium Hydroxide → HCID 19418871、化合物
反応式
[Br:1][C:2]1[C:3]([O:15][CH3:16])=[CH:4][CH:5]=[C:6]2[C:10]=1[NH:9][C:8]([C:11]([O:13]C)=[O:12])=[CH:7]2.[OH-].[K+]>>[Br:1][C:2]1[C:3]([O:15][CH3:16])=[CH:4][CH:5]=[C:6]2[C:10]=1[NH:9][C:8]([C:11]([OH:13])=[O:12])=[CH:7]2参加物
3
実験手順
Following the general procedure of PREPARATION 63 and making non-critical variations but starting with methyl 7-bromo-6-methoxyindole carboxylate (PREPARATION 81, 0.36 g) and potassium hydroxide (0.11 g), the title compound is obtained, NMR (300 MHz, CD3OD), 7.58, 7.20, 6.96 and 3.93 δ.
後処理
- customthe general procedure of PREPARATION 63
出典と根拠
- ORDレコード
- ord-82efb92adb9a470ead805f5bf6fbd8f8
- 出典データセット
- uspto-grants-1996_02
- 特許番号
- US05489593
反応ノート
読み込み中…