化工社化工社 化学情報印刷レポート · 研究参考用
Dimethylformamide → 2,2',4,4'-Tetrahydroxybenzophenone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dimethylformamide | HCID 6228 | — |
| 反応物 | Benzophenone-6 | HCID 8570 | — |
| 反応物 | Aluminum(III) Chloride | HCID 6451240 | — |
| 生成物 | 2,2',4,4'-Tetrahydroxybenzophenone | HCID 8571 | — |
反応手順
82.2 g (0.30 mol) of 2,2'-dihydroxy-4,4'-dimethoxybenzophenone were reacted with 600 g of AlCl3 (4.50 mol) and 180 g (2.47 mol) of DMF (dimethylformamide) as in Example 2, and the product was worked up as described.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05728888 |
| 出典データセット | uspto-grants-1998_03 |
| ORD ID | ord-3dda345d3c8b43eca91644036bf8ff3e |
| 出典メモ | uspto-grants-1998_03 |