Ethanol → Ethyl sulfoacetate

HRID 2396092

反応式

HRID 2396092 の反応式
[S:1]([CH2:5][C:6]([OH:8])=[O:7])([OH:4])(=[O:3])=[O:2].[CH3:9][CH2:10]O>>[S:1]([CH2:5][C:6]([O:8][CH2:9][CH3:10])=[O:7])([OH:4])(=[O:3])=[O:2]

参加物

3

反応物 2

HCID 702EthanolHCID 31257Sulfoacetic acid

生成物 1

HCID 12216623Ethyl sulfoacetate

実験手順

Sulfoacetic acid (52 g, 371 mM) and EtOH (500 mL) were heated under reflux for 20 hours. The reaction mixture was cooled, and the excess ethanol was removed under vacuum to give ethyl sulfoacetate.

後処理

  1. temperatureunder reflux for 20 hours
  2. temperatureThe reaction mixture was cooled
  3. customthe excess ethanol was removed under vacuum

出典と根拠

ORDレコード
ord-292b72945d0e454c82fdb19175274c63
出典データセット
uspto-grants-1996_02
特許番号
US05491170

関連ノート

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