HCID 10279786、化合物 → HCID 10110008、化合物
反応式
CC([C:4]1[CH:9]=[C:8](C(C)C)[CH:7]=[C:6](C(C)C)[C:5]=1[CH2:16][C:17]([C:19]1[C:20]([CH:33]([CH3:35])[CH3:34])=[C:21]([O:28][S:29](=[O:32])(=[O:31])[NH2:30])[C:22]([CH:25]([CH3:27])[CH3:26])=[CH:23][CH:24]=1)=[O:18])C.C(C1C=C(C(C)C)C=C(C(C)C)C=1C[Mg]Br)(C)C.C([Mg]Cl)C1C=CC=CC=1>>[C:5]1([CH2:16][C:17]([C:19]2[C:20]([CH:33]([CH3:35])[CH3:34])=[C:21]([O:28][S:29](=[O:31])(=[O:32])[NH2:30])[C:22]([CH:25]([CH3:27])[CH3:26])=[CH:23][CH:24]=2)=[O:18])[CH:6]=[CH:7][CH:8]=[CH:9][CH:4]=1参加物
4
実験手順
This compound was prepared in the same manner as the title compound of Example 5, except that 2,4,6-triisopropylbenzyl magnesium bromide was replaced with benzylmagnesium chloride (commercially available), mp 150°-152° C.
出典と根拠
- ORDレコード
- ord-ad3f0f43e1f04de2ab2e5a67bd352e9b
- 出典データセット
- uspto-grants-1996_02