1,3-Propanediamine → N,N'-(1,3-propylene)-bis[2-hydroxyundecylamine]
反応式
[CH2:1]1[O:12][CH:2]1[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH3:11].[CH2:13]([NH2:17])[CH2:14][CH2:15][NH2:16]>CO>[CH2:13]([NH:17][CH2:1][CH:2]([OH:12])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH3:11])[CH2:14][CH2:15][NH:16][CH2:1][CH:2]([OH:12])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH3:11]参加物
4
実験手順
In a manner similar to that of Example 1, condensation of 1-undecene oxide (104.6 g.) and 1,3-propanediamine (22.7 g.) and two recrystallizations of the resulting product from methanol gave N,N'-(1,3-propylene)-bis[2-hydroxyundecylamine] (I: R= CH3 (CH2)8, R' = H, X= (CH2)3, Z= H) (29.0 g., m.p. 94.0°-103.0° C.).
出典と根拠
- ORDレコード
- ord-5d2ccff6c27d46b8a4ccfdf32b8efce1
- 出典データセット
- uspto-grants-1977_05