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2,6-Dimethylbenzoyl chloride → Benzamide, 2,6-dimethyl-N-(1,2,3,4-tetrahydro-2-methylisoquinolin-5-yl)-
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2,6-Dimethylbenzoyl chloride | HCID 89096 | — |
| 反応物 | 2-Methyl-1,2,3,4-tetrahydroisoquinolin-5-amine | HCID 14171269 | — |
| 生成物 | Benzamide, 2,6-dimethyl-N-(1,2,3,4-tetrahydro-2-methylisoquinolin-5-yl)- | HCID 216597 | — |
反応手順
5-Amino-2-methyl-1,2,3,4-tetrahydroisoquinoline was reacted with 2,6-dimethylbenzoyl chloride according to the procedure of Example 19 to yield 5-(2,6-dimethylbenzamido)-2-methyl-1,2,3,4-tetrahydroisoquinoline; m.p. 199.5°-201° C. after purification from ethanol.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04022900 |
| 出典データセット | uspto-grants-1977_05 |
| ORD ID | ord-a52bcd0ba2484e159f9810754ee83fba |
| 出典メモ | uspto-grants-1977_05 |