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Methyl N-cyanocarbamate → 5-Cyclohexylethylthio-2-carbomethoxyaminobenzimidazole
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methyl N-cyanocarbamate | HCID 89023 | — |
| 反応物 | 2-Nitro-5-cyclohexylethylthioaniline | HCID 54479877 | — |
| 生成物 | 5-Cyclohexylethylthio-2-carbomethoxyaminobenzimidazole | HCID 54415697 | — |
反応手順
Repeating the reaction of Example 1 but using 10.0 g. of cyclohexylethylthiol gives 2-nitro-5-cyclohexylethylthioaniline. The nitro compound is reduced. The reduction mixture is reacted with carbomethoxycyanamide as described to give 5-cyclohexylethylthio-2-carbomethoxyaminobenzimidazole.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04025638 |
| 出典データセット | uspto-grants-1977_05 |
| ORD ID | ord-daa640345104442a88f6a1a9fd58de27 |
| 出典メモ | uspto-grants-1977_05 |