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2-Amino-5-bromopyridine → N-(5-bromopyridin-2-yl)-N'-(2-fluoro-5-methylphenyl)urea
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Amino-5-bromopyridine | HCID 70622 | — |
| 反応物 | 3-Fluorophenyl isocyanate | HCID 123064 | — |
| 反応物 | 2-Fluoro-5-methylphenyl isocyanate | HCID 2733377 | — |
| 生成物 | N-(5-bromopyridin-2-yl)-N'-(2-fluoro-5-methylphenyl)urea | HCID 66680783 | — |
反応手順
The desired product was prepared by substituting 2-amino-5-bromopyridine and 1-fluoro-2-isocyanato-4-methylbenzene for Example 15G and 1-fluoro-3-isocyanatobenzene, respectively, in Example 15H. MS (ESI(+)) m/e 324.0 (M+H)+.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08642776B2 |
| 出典データセット | uspto-grants-2014_02 |
| ORD ID | ord-562fd293a52f4ba0aee10c7fb26adb85 |
| 出典メモ | uspto-grants-2014_02 |