化工社化工社 化学情報印刷レポート · 研究参考用
1-Chlorooctadecane → Stearyl-[3-(p-Dimethylaminobenzamido)propyl]-Dimethylammonium Chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Chlorooctadecane | HCID 18815 | — |
| 反応物 | 4-(dimethylamino)-N-[3-(dimethylamino)propyl]benzamide | HCID 3978888 | — |
| 生成物 | Stearyl-[3-(p-Dimethylaminobenzamido)propyl]-Dimethylammonium Chloride | HCID 67735953 | — |
反応手順
25.6 g of N-(3-dimethylaminopropyl)-p-dimethylaminobenzamide (0.103 mole) from Example 1 and 28.6 g of stearylchloride (0.099 mole) were melted together and kept at 130° C. for 3 hours. Product was crystallized from 250 ml of methylethylketone. Yield was 42 g (77% of theoretical yield).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05451394 |
| 出典データセット | uspto-grants-1995_09 |
| ORD ID | ord-c2948ff93b0a4e79828553c13ad7a958 |
| 出典メモ | uspto-grants-1995_09 |