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Myristyl chloride → Tetradecyl-[3-(p-Dimethylaminobenzamido)propyl]-Dimethylammonium Chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Myristyl chloride | HCID 17043 | — |
| 反応物 | 4-(dimethylamino)-N-[3-(dimethylamino)propyl]benzamide | HCID 3978888 | — |
| 生成物 | Tetradecyl-[3-(p-Dimethylaminobenzamido)propyl]-Dimethylammonium Chloride | HCID 15825621 | — |
反応手順
50 g of N-(3-dimethylaminopropyl)-p-dimethylaminobenzamide (0.201 mole) from Example 1 and 47 g of tetradecylchloride (0.195 mole) were melted together and kept at 130° C. for 4 hours. Product was crystallized from 250 ml of ethylacetate; the crystals were washed with another 150 ml of ethylacetate. Yield was 71 g (74% of theoretical yield).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05451394 |
| 出典データセット | uspto-grants-1995_09 |
| ORD ID | ord-caf60ebe87a6448e9d4e4e1649dbf069 |
| 出典メモ | uspto-grants-1995_09 |