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3,4-Dichloro-N-methylaniline → HCID 57444242、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3,4-Dichloro-N-methylaniline | HCID 2800931 | — |
| 反応物 | N-{3-[4-(chloromethyl)phenyl]pyrazin-2-yl}-2-(trifluoromethyl)benzenesulfonamide | HCID 57444250 | — |
| 生成物 | HCID 57444242 | HCID 57444242 | 63% |
反応手順
Following the general method as outlined in Example 1 (Method B), starting from N-{3-[4-(chloromethyl)phenyl]pyrazin-2-yl}-2-(trifluoromethyl)benzenesulfonamide (Intermediate 9), and 3,4-dichloro-N-methylaniline, the title compound was isolated as a yellow solid in 63% yield (91% purity by HPLC).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08796280B2 |
| 出典データセット | uspto-grants-2014_08 |
| ORD ID | ord-3932349de9894e09bfb77e40a090d87d |
| 出典メモ | uspto-grants-2014_08 |