化工社化工社 化学情報印刷レポート · 研究参考用
Hydrochloric Acid → HCID 178510555、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | 9-oxo-9H-indeno(1,2-b)pyrazine-2,3-dicarbonitrile | HCID 292929 | — |
| 生成物 | HCID 178510555 | HCID 178510555 | 90% |
反応手順
A suspension of 1 (5.66 g, 24.3 mmol) in aqueous NaOH (2% w/v, 81 ml) was stirred at room temperature for 16 hours. The mixture was acidified with 3N HCl to pH 1, the precipitate was collected by filtration, washed with water and dried under vacuum, affording 6 (4.88 g, 90%) as light brown solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08648076B2 |
| 出典データセット | uspto-grants-2014_02 |
| ORD ID | ord-4af3784d1a4c4d8a8ef952e3236eaa83 |
| 出典メモ | uspto-grants-2014_02 |