Benzoic Acid → HCID 178443205、化合物

HRID 2403125

反応式

HRID 2403125 の反応式
[CH3:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][N+:14]([CH2:17][C:18]1[CH:19]=[CH:20][CH:21]=[CH:22][CH:23]=1)([CH3:16])[CH3:15].[C:24]([OH:32])(=[O:31])[C:25]1[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=1.[OH2:33]>CC(C)=O>[CH3:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][N+:14]([CH2:17][C:18]1[CH:19]=[CH:20][CH:21]=[CH:22][CH:23]=1)([CH3:16])[CH3:15].[C:24]([O-:32])(=[O:31])[C:25]1[C:30](=[CH:29][CH:28]=[CH:27][CH:26]=1)[OH:33]

参加物

5

反応物 3

HCID 243Benzoic AcidHCID 962WaterHCID 2330Benzalkonium

生成物 1

HCID 178443205HCID 178443205、化合物

試薬・触媒・溶媒 1

HCID 180Acetone溶媒

実験手順

Benzalkonium saccharinate (0.01 mol) and benzoic acid (0.01 mol) were dissolved in 25 mL of hot acetone. The mixture was stirred at room temperature for 5 h. Distilled water was added. The organic phase was separated and washed with distilled water. Organic phase was evaporated and the product, benzalkonium salicylate, was dried under vacuum. 1H and 13C NMR (DMSO) were obtained.

後処理

  1. customThe organic phase was separated
  2. washwashed with distilled water
  3. customOrganic phase was evaporated
  4. dry with materialthe product, benzalkonium salicylate, was dried under vacuum
  5. custom1H and 13C NMR (DMSO) were obtained

出典と根拠

ORDレコード
ord-3323f506f78c4f2ca2530abb2a35cff9
出典データセット
uspto-grants-2014_08
特許番号
US08802596B2

関連ノート

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