Formamide → HCID 178518065、化合物
反応式
C([O:3][C:4]([C:6]1[C:7]2[CH:15]=[CH:14][CH:13]=[CH:12][C:8]=2[S:9][C:10]=1[NH2:11])=O)C.[CH:16]([NH2:18])=O>>[N:11]1[C:10]2[S:9][C:8]3[CH:12]=[CH:13][CH:14]=[CH:15][C:7]=3[C:6]=2[C:4]([OH:3])=[N:18][CH:16]=1参加物
3
実験手順
The solution of 10 millimol IX in 15 milliliter milliliter formamide was stirred at 100° C. for 3 hours then cooled down to room temperature. The reaction mixture was poured onto crushed ice with continuous stirring then collected by filtration. The product was washed with water and n-hexane, then dried.
後処理
- additionThe reaction mixture was poured
- customonto crushed ice
- filtrationthen collected by filtration
- washThe product was washed with water and n-hexane
- customdried
出典と根拠
- ORDレコード
- ord-fcd1f227558b4307b108c50fdc9d3f9d
- 出典データセット
- uspto-grants-2014_08
- 特許番号
- US08802849B2
反応ノート
読み込み中…