4-Bromobenzaldehyde → HCID 68543749、化合物
反応式
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([C:8](=[O:22])[CH2:9][S:10]([CH2:13][C:14]2[CH:19]=[CH:18][C:17]([O:20][CH3:21])=[CH:16][CH:15]=2)(=[O:12])=[O:11])=[CH:4][CH:3]=1.[Br:23][C:24]1[CH:31]=[CH:30][C:27]([CH:28]=O)=[CH:26][CH:25]=1>>[Br:1][C:2]1[CH:3]=[CH:4][C:5]([C:8](=[O:22])/[C:9](/[S:10]([CH2:13][C:14]2[CH:15]=[CH:16][C:17]([O:20][CH3:21])=[CH:18][CH:19]=2)(=[O:11])=[O:12])=[CH:28]\[C:27]2[CH:30]=[CH:31][C:24]([Br:23])=[CH:25][CH:26]=2)=[CH:6][CH:7]=1参加物
3
実験手順
The title compound is prepared by the methods described in Synthesis Example 10. A solution of 1-(4-bromophenyl)-2-(4-methoxybenzylsulfonyl)ethanone (10 mmol) and 4-bromobenzaldehyde (10 mmol) was subjected to the procedure described as Method A in part C of Synthesis Example 10 and the product obtained was purified by column chromatography. m.p. 146-150° C.
後処理
- customdescribed in Synthesis Example 10
- customdescribed as Method A in part C of Synthesis Example 10
- customthe product obtained
- customwas purified by column chromatography