4-Iodobenzaldehyde → HCID 68539858、化合物

HRID 2405547ノート

反応式

HRID 2405547 の反応式
[I:1][C:2]1[CH:7]=[CH:6][C:5]([C:8](=[O:21])[CH2:9][S:10]([CH2:13][C:14]2[CH:19]=[CH:18][C:17]([I:20])=[CH:16][CH:15]=2)(=[O:12])=[O:11])=[CH:4][CH:3]=1.[I:22][C:23]1[CH:30]=[CH:29][C:26]([CH:27]=O)=[CH:25][CH:24]=1>>[I:1][C:2]1[CH:3]=[CH:4][C:5]([C:8](=[O:21])/[C:9](/[S:10]([CH2:13][C:14]2[CH:19]=[CH:18][C:17]([I:20])=[CH:16][CH:15]=2)(=[O:11])=[O:12])=[CH:27]\[C:26]2[CH:29]=[CH:30][C:23]([I:22])=[CH:24][CH:25]=2)=[CH:6][CH:7]=1

参加物

3

反応物 2

HCID 966574-IodobenzaldehydeHCID 68543718HCID 68543718、化合物

生成物 1

HCID 68539858HCID 68539858、化合物

実験手順

The title compound is prepared by the methods described in Synthesis Example 10. A solution of 1-(4-iodophenyl)-2-(4-iodobenzylsulfonyl)ethanone (10 mmol) and 4-iodobenzaldehyde (10 mmol) was subjected to the procedure described as Method A in part C of Synthesis Example 10 and the product obtained was purified by column chromatography.

後処理

  1. customdescribed in Synthesis Example 10
  2. customdescribed as Method A in part C of Synthesis Example 10
  3. customthe product obtained
  4. customwas purified by column chromatography

出典と根拠

ORDレコード
ord-5693be8ee7b045e5962ebcc84560209c
出典データセット
uspto-grants-2014_08
特許番号
US08808702B2

反応ノート

読み込み中…