関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 2-Amino-5-nitrobenzoic acid | HCID 12032 | — |
| 反応物 | Formamidine acetate | HCID 160693 | — |
| 溶媒 | 1-Methoxyethanol | HCID 3015637 | — |
| 生成物 | HCID 178526470 | HCID 178526470 | — |
反応手順
A mixture of 2-amino-5-nitrobenzoic acid (1000 g, 5 mol) and formamidine acetate (1000 g, 10 mol) were dissolved in methoxyethanol (4 L) and heated to 115° C. for 16 hours. After cooling the mixture to room temperature, ice water (5 L) was added and the mixture was stirred for 30 minutes before collecting the product (125 g, 14%) by filtration.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US08648087B2 |
|---|
| 出典データセット | uspto-grants-2014_02 |
|---|
| ORD ID | ord-c6eaa425e0df4e24ab878d970d8aa4c3 |
|---|
| 出典メモ | uspto-grants-2014_02 |
|---|
