関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Formamide | HCID 713 | — |
| 反応物 | Benzoic acid, 2-amino-5-iodo- | HCID 72911 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | HCID 178518013 | HCID 178518013 | 83% |
反応手順
A mixture of 2-amino-5-iodobenzoic acid (125 g, 475 mmol) and formamide (200 mL) was heated to 190° C. for 2 hours. After cooling to room temperature, the reaction mixture was poured into water (500 mL) and stirred for 2 hours. The solids were filtered and dried under high vacuum to provide the product (108 g, 83%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US08648087B2 |
|---|
| 出典データセット | uspto-grants-2014_02 |
|---|
| ORD ID | ord-1cf203d6a8f34d2ea4d9ba40e1884b22 |
|---|
| 出典メモ | uspto-grants-2014_02 |
|---|
