Phenylsulfamate → HCID 57785269、化合物

反応式

[C:1]1([O:7][S:8](=[O:11])(=[O:10])[NH2:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.C(C1(O)CC1)CC>>[CH2:6]([C:1]1([O:7][S:8](=[O:10])(=[O:11])[NH2:9])[CH2:2][CH2:3]1)[CH2:5][CH3:4]

参加物

反応物 2

HCID 11030308Phenylsulfamate

HCID 130466221-Propylcyclopropanol

生成物 1

HCID 57785269HCID 57785269、化合物

実験手順

Sulfamic acid 1-propyl-cyclopropyl ester was synthesized according to the method presented in the synthesis of sulfamic acid phenyl ester in Example 1 with the exception of utilizing 1-propylcyclopropanol (synthesized by methods reported in Synthesis 1991, 234) to obtain sulfamic acid 1-propyl-cyclopropyl ester.

後処理

customSulfamic acid 1-propyl-cyclopropyl ester was synthesized

出典と根拠

ORDレコード: ord-05646e9f523b4a268c982ea03ec29914
出典データセット: uspto-grants-2014_08
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US08809267B2

反応ノート

読み込み中…