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tert-Butyl pyrazolidine-1-carboxylate → t-Butyl 2-[(5-(4-chlorophenyl)-6-(2,2,2-trifluoroethoxy)-3-pyridinyl)carbonyl]-pyrazolidine-1-carboxylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | tert-Butyl pyrazolidine-1-carboxylate | HCID 21857793 | — |
| 反応物 | 5-(4-Chloro-phenyl)-6-(2,2,2-trifluoro-ethoxy)-nicotinic acid | HCID 66686971 | — |
| 生成物 | t-Butyl 2-[(5-(4-chlorophenyl)-6-(2,2,2-trifluoroethoxy)-3-pyridinyl)carbonyl]-pyrazolidine-1-carboxylate | HCID 71294447 | — |
反応手順
The title compound was synthesized in analogy to Example 1 using 5-(4-chlorophenyl)-6-(2,2,2-trifluoroethoxy)-3-pyridinecarboxylic acid (CAN 1018782-82-5) and 1-pyrazolidinecarboxylic acid 1,1-dimethylethyl ester (CAN 57699-91-9) as starting materials; MS (EI) 486.2 (M+H)+.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08648099B2 |
| 出典データセット | uspto-grants-2014_02 |
| ORD ID | ord-13ad7180d565474e85d2285da3b37b3a |
| 出典メモ | uspto-grants-2014_02 |