化工社化工社 化学情報印刷レポート · 研究参考用
N-methyl-N-phenyl-hydrazine → 5-(4-chloro-phenyl)-6-(2,2,2-trifluoro-ethoxy)-3-pyridinecarboxylic acid N'-methyl-N'-phenyl-hydrazide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N-methyl-N-phenyl-hydrazine | HCID 36299 | — |
| 反応物 | 5-(4-Chloro-phenyl)-6-(2,2,2-trifluoro-ethoxy)-nicotinic acid | HCID 66686971 | — |
| 生成物 | 5-(4-chloro-phenyl)-6-(2,2,2-trifluoro-ethoxy)-3-pyridinecarboxylic acid N'-methyl-N'-phenyl-hydrazide | HCID 71294427 | — |
反応手順
The title compound was synthesized in analogy to Example 1 using 5-(4-chlorophenyl)-6-(2,2,2-trifluoroethoxy)-3-pyridinecarboxylic acid (CAN 1018782-82-5) and 1-methyl-1-phenyl-hydrazine (CAN 618-40-6) as starting materials; MS (EI) 436.3 (M+H)+.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08648099B2 |
| 出典データセット | uspto-grants-2014_02 |
| ORD ID | ord-7c8b2c96f5f84582ab96174c654b13c2 |
| 出典メモ | uspto-grants-2014_02 |