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N-methyl-N-phenyl-hydrazine → 5-cyclopentyl-N'-methyl-N'-phenyl-6-(2,2,2-trifluoroethoxy)-3-pyridinecarboxylic acid hydrazide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N-methyl-N-phenyl-hydrazine | HCID 36299 | — |
| 反応物 | 5-Cyclopentyl-6-(2,2,2-trifluoroethoxy)-3-pyridinecarboxylic acid | HCID 71294186 | — |
| 生成物 | 5-cyclopentyl-N'-methyl-N'-phenyl-6-(2,2,2-trifluoroethoxy)-3-pyridinecarboxylic acid hydrazide | HCID 71294058 | — |
反応手順
The title compound was synthesized in analogy to Example 1 using 5-cyclopentyl-6-(2,2,2-trifluoro-ethoxy)-3-pyridinecarboxylic acid (example 14c) and 1-methyl-1-phenyl-hydrazine (CAN 618-40-6) as starting materials; LC-MS (UV peak area/ESI) 98.0%, 394.1737 (M+H)+.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08648099B2 |
| 出典データセット | uspto-grants-2014_02 |
| ORD ID | ord-196e0bc19b5941eb8d3a2be5fcd72ade |
| 出典メモ | uspto-grants-2014_02 |