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HRID 240712作成日：2026年10月26日

3-Chloro-6-(1-methylhydrazinyl)pyridazine → N'-(6-chloropyridazin-3-yl)-5-cyclohexyl-N'-methyl-6-(2,2,2-trifluoroethoxy)-3-pyridinecarboxylic acid hydrazide

https://huagongshe.com/reaction/240712

反応式

関与物質

役割名称HCID仕込み量
反応物3-Chloro-6-(1-methylhydrazinyl)pyridazineHCID 2735815—
反応物5-Cyclohexyl-6-(2,2,2-trifluoroethoxy)nicotinic acidHCID 71293952—
生成物N'-(6-chloropyridazin-3-yl)-5-cyclohexyl-N'-methyl-6-(2,2,2-trifluoroethoxy)-3-pyridinecarboxylic acid hydrazideHCID 71510018—

反応手順

The title compound was synthesized in analogy to Example 1 using 5-cyclohexyl-6-(2,2,2-trifluoro-ethoxy)-3-pyridinecarboxylic acid (example 12c) and 3-chloro-6-(1-methylhydrazinyl)-pyridazine (CAN 76953-33-8) as starting materials; LC-MS (UV peak area/ESI) 100.0%, 444.1408 (M+H)+.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US08648099B2
出典データセットuspto-grants-2014_02
ORD IDord-c7435d94371f4c3f948f87b282b5308f
出典メモuspto-grants-2014_02