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N-methyl-N-phenyl-hydrazine → 5-cyclopropyl-6-(2,2,2-trifluoro-ethoxy)-nicotinic acid N'-methyl-N'-phenyl-hydrazide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N-methyl-N-phenyl-hydrazine | HCID 36299 | — |
| 反応物 | 5-Cyclopropyl-6-(2,2,2-trifluoroethoxy)nicotinic acid | HCID 71294108 | — |
| 生成物 | 5-cyclopropyl-6-(2,2,2-trifluoro-ethoxy)-nicotinic acid N'-methyl-N'-phenyl-hydrazide | HCID 71294365 | — |
反応手順
The title compound was synthesized in analogy to the procedure described in Example 34 c), using 5-cyclopropyl-6-(2,2,2-trifluoro-ethoxy)-nicotinic acid (example 34b) and N-methyl-N-phenyl-hydrazine (CAN 618-40-6); MS (ESI) 366.2 (M+H)+.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08648099B2 |
| 出典データセット | uspto-grants-2014_02 |
| ORD ID | ord-9db011e11dfb413f88b43d4dfe9e5ff4 |
| 出典メモ | uspto-grants-2014_02 |