tert-Octylamine → HCID 86656469、化合物

反応式

[N:1]([CH2:4][CH2:5][C:6]1[S:7][CH:8]=[CH:9][CH:10]=1)=[C:2]=[S:3].[C:11]([NH2:19])([CH2:14][C:15]([CH3:18])([CH3:17])[CH3:16])([CH3:13])[CH3:12]>>[C:11]([NH:19][C:2]([NH:1][CH2:4][CH2:5][C:6]1[S:7][CH:8]=[CH:9][CH:10]=1)=[S:3])([CH2:14][C:15]([CH3:18])([CH3:17])[CH3:16])([CH3:13])[CH3:12]

参加物

反応物 2

HCID 61017tert-Octylamine

HCID 101763092-(2-Isothiocyanatoethyl)thiophene

生成物 1

HCID 86656469HCID 86656469、化合物収率 83%

実験手順

The procedure of step (1-1) of Example 1 was repeated except for using the compound obtained in step (2-1) (2.5 g, 15.0 mmol) and t-octyl amine (1.6 mL, 10.2 mmol), to obtain the title compound (2.5 g, 83%).

出典と根拠

ORDレコード: ord-c833821c4062406bbd394a19d3e2b44e
出典データセット: uspto-grants-2014_02
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US08648111B2

反応ノート

読み込み中…