Vanillylmandelic Acid → N-heptyl-2-hydroxy-2-(4-hydroxy-3-methoxyphenyl)acetamide

HRID 2410617

反応式

HRID 2410617 の反応式
[OH:1][C:2]1[CH:12]=[CH:11][C:5]([CH:6]([OH:10])[C:7]([OH:9])=O)=[CH:4][C:3]=1[O:13][CH3:14].[CH2:15]([NH2:22])[CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH3:21].CCCC(NC(=O)C(O)C1C=CC(O)=C(OC)C=1)CCC>>[CH2:15]([NH:22][C:7](=[O:9])[CH:6]([OH:10])[C:5]1[CH:11]=[CH:12][C:2]([OH:1])=[C:3]([O:13][CH3:14])[CH:4]=1)[CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH3:21]

参加物

4

実験手順

N-heptyl-2-hydroxy-2-(4-hydroxy-3-methoxyphenyl)acetamide was prepared from 4-hydroxy-3-methoxymandelic acid and n-heptylamine by the same procedure described for the preparation of N-(heptan-4-yl)-2-hydroxy-2-(4-hydroxy-3-methoxyphenyl)acetamide. White crystals of the title compound (6.7 g, 89% yield) were obtained.

出典と根拠

ORDレコード
ord-2fb8963808e944b38a86ad8da0970f8c
出典データセット
uspto-grants-2014_08
特許番号
US08816102B2

関連ノート

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