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6-Bromonicotinic acid → (6-Bromopyridin-3-yl)[4-(p-tolyloxy)piperidin-1-yl]methanone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 6-Bromonicotinic acid | HCID 238932 | — |
| 反応物 | 4-(4-Methylphenoxy)piperidine | HCID 3837497 | — |
| 生成物 | (6-Bromopyridin-3-yl)[4-(p-tolyloxy)piperidin-1-yl]methanone | HCID 58484591 | 99.9% |
反応手順
Using 4-(p-tolyloxy)piperidine (765 mg) and 6-bromonicotinic acid (808 mg) and by the reaction and treatment in the same manner as in Preparation Example 118, the title compound (1.5 g) was obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08816079B2 |
| 出典データセット | uspto-grants-2014_08 |
| ORD ID | ord-e46681dc325d47bfaf2d19e9ad6d59c7 |
| 出典メモ | uspto-grants-2014_08 |