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2-(Trifluoromethyl)aniline → 4-methoxy-N-[2-(trifluoromethyl)phenyl]benzenesulfonamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-(Trifluoromethyl)aniline | HCID 6922 | — |
| 反応物 | 4-Methoxybenzenesulfonyl chloride | HCID 7401 | — |
| 生成物 | 4-methoxy-N-[2-(trifluoromethyl)phenyl]benzenesulfonamide | HCID 755970 | 75.5% |
反応手順
Using 2-trifluoromethylaniline (1.39 g, 8.55 mmol) and 4-methoxybenzenesulfonyl chloride (1.78 g, 8.55 mmol), the procedure of Reference Example 2 was repeated to obtain 2.14 g (75.5%) of the title compound in the form of colorless solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05728835 |
| 出典データセット | uspto-grants-1998_03 |
| ORD ID | ord-a203f03510c84376936109923b3e225b |
| 出典メモ | uspto-grants-1998_03 |