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2-Amino-2-methyl-1,3-propanediol → [2-(Chrysen-2-ylmethylamino)-3-hydroxy-2-methylpropyl] methanesulfonate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Amino-2-methyl-1,3-propanediol | HCID 1531 | — |
| 反応物 | Chrysene-2-carbaldehyde | HCID 15599322 | — |
| 反応物 | 2-((6-Chrysenylmethyl)amino)-2-methyl-1,3-propanediol methanesulfonate | HCID 54096087 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | [2-(Chrysen-2-ylmethylamino)-3-hydroxy-2-methylpropyl] methanesulfonate | HCID 54052581 | — |
反応手順
Using the reductive amination procedure outlined in 1C, chrysene-2-carbaldehyde (20D) and 2-amino-2-methyl-1,3-propanediol (Aldrich) gave 2-((2-chrysenylmethyl)amino)-2-methyl-1,3-propanediol methanesulfonate, mp 225°-227° (dec), (abs. EtOH), (C, H, N, S)
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04719046 |
| 出典データセット | uspto-grants-1988_01 |
| ORD ID | ord-26d51dc902e640c5921dda0a3e3876b5 |
| 出典メモ | uspto-grants-1988_01 |