Phosphinic acid, P-phenyl-P-(2,4,6-trimethylbenzoyl)-, sodium salt (1:1) → Phenyl(2,4,6-trimethylbenzoyl)phosphinate

HRID 2413830ノート

反応式

HRID 2413830 の反応式
[CH3:1][C:2]1[CH:18]=[C:17]([CH3:19])[CH:16]=[C:15]([CH3:20])[C:3]=1[C:4]([P:6]([C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1)(=[O:8])[O-:7])=[O:5].[Na+]>O.S(=O)(=O)(O)O>[CH3:1][C:2]1[CH:18]=[C:17]([CH3:19])[CH:16]=[C:15]([CH3:20])[C:3]=1[C:4]([P:6]([C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1)(=[O:7])[OH:8])=[O:5]

参加物

4

反応物 1

HCID 23690966Phosphinic acid, P-phenyl-P-(2,4,6-trimethylbenzoyl)-, sodium salt (1:1)

生成物 1

HCID 18674595Phenyl(2,4,6-trimethylbenzoyl)phosphinate

試薬・触媒・溶媒 2

HCID 962Water溶媒HCID 1118Sulfuric Acid溶媒

実験手順

46.5 parts by weight of the sodium salt of Example 1 were dissolved in 300 parts by weight of water, and 150 parts by volume of 1N sulfuric acid were added. The resulting precipitate was filtered off under suction, washed with water and dried, and 38.9 parts by weight of product were obtained.

後処理

  1. additionwere added
  2. filtrationThe resulting precipitate was filtered off under suction
  3. washwashed with water
  4. customdried
  5. custom38.9 parts by weight of product were obtained

出典と根拠

ORDレコード
ord-2fa8484411324ff68d11f97931f1101c
出典データセット
uspto-grants-1988_01
特許番号
US04719297

反応ノート

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