Calcium Chloride → HCID 88641856、化合物

HRID 2413831ノート

反応式

HRID 2413831 の反応式
[CH3:1][C:2]1[CH:18]=[C:17]([CH3:19])[CH:16]=[C:15]([CH3:20])[C:3]=1[C:4]([P:6]([C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1)(=[O:8])[O-:7])=[O:5].[Na+].[Cl-].[Ca+2:23].[Cl-]>O>[CH3:1][C:2]1[CH:18]=[C:17]([CH3:19])[CH:16]=[C:15]([CH3:20])[C:3]=1[C:4]([P:6]([C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1)(=[O:7])[O-:8])=[O:5].[CH3:1][C:2]1[CH:18]=[C:17]([CH3:19])[CH:16]=[C:15]([CH3:20])[C:3]=1[C:4]([P:6]([C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1)(=[O:7])[O-:8])=[O:5].[Ca+2:23]

参加物

4

反応物 2

HCID 5284359Calcium ChlorideHCID 23690966Phosphinic acid, P-phenyl-P-(2,4,6-trimethylbenzoyl)-, sodium salt (1:1)

生成物 1

HCID 88641856HCID 88641856、化合物

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

15 parts by weight of the sodium salt of Example 1 were dissolved in 75 parts by weight of water, and 125 parts by volume of a 10% strength aqueous calcium chloride solution were added a little at a time to this solution. The resulting precipitate was filtered off under suction, washed with water and dried in a drying oven under reduced pressure at 50° C., and 14.7 parts by weight of product were obtained.

後処理

  1. additionwere added a little at a time to this solution
  2. filtrationThe resulting precipitate was filtered off under suction
  3. washwashed with water
  4. customdried in a drying oven under reduced pressure at 50° C.
  5. custom14.7 parts by weight of product were obtained

出典と根拠

ORDレコード
ord-bf4042638b344e4c9bd77cf614fc03a9
出典データセット
uspto-grants-1988_01
特許番号
US04719297

反応ノート

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