4-Methyl-2-pentylpyridine → HCID 67451102、化合物

HRID 241483ノート

反応式

HRID 241483 の反応式
C[C:2]1[CH:7]=[CH:6]N=[C:4]([CH2:8]CCCC)[CH:3]=1.C([Mg]Br)CCCCC.Cl[C:22]1[CH:27]=[C:26]([CH2:28][CH3:29])[CH:25]=[CH:24][N:23]=1>>[CH2:28]([C:26]1[CH:25]=[CH:24][N:23]=[C:22]([CH2:6][CH2:7][CH2:2][CH2:3][CH2:4][CH3:8])[CH:27]=1)[CH3:29]

参加物

4

反応物 3

HCID 30200104-Methyl-2-pentylpyridineHCID 36534732-Chloro-4-ethylpyridineHCID 178444609HCID 178444609、化合物

生成物 1

HCID 67451102HCID 67451102、化合物

実験手順

This compound was obtained using the same experimental procedure as per 4-methyl-2-pentyl-pyridine (see above), using hexyl magnesium bromide instead of pentyl magnesium bromide and 2-chloro-4-ethyl pyridine instead of 2-bromo-4-methylpyridine. The product was obtained with similar yield and purified in the same way.

後処理

  1. customThis compound was obtained
  2. customThe product was obtained
  3. customwith similar yield
  4. custompurified in the same way

出典と根拠

ORDレコード
ord-1b440411a4b44ef8859a5c6b53b24894
出典データセット
uspto-grants-2014_02
特許番号
US08652452B2

反応ノート

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